Post 412790 (https://www.thevespiary.org/talk/index.php?topic=11997.msg41279000#msg41279000)
(Lego: "Betaine for O-methylation of Phenols", Novel Discourse)Post 418138 (https://www.thevespiary.org/talk/index.php?topic=11802.msg41813800#msg41813800)
(bottleneck: "Etherification by cat. amounts of a tosylate?", Novel Discourse)Post 417550 (https://www.thevespiary.org/talk/index.php?topic=11342.msg41755000#msg41755000)
(Antoncho: "Methyl tosylate: _finally_ , OTC!!!", Novel Discourse)Post 398206 (https://www.thevespiary.org/talk/index.php?topic=11534.msg39820600#msg39820600)
(GC_MS: "Electrosynthesis of gamma-asarone", Novel Discourse)Post 398635 (https://www.thevespiary.org/talk/index.php?topic=11534.msg39863500#msg39863500)
(Mountain_Girl: "Methyl Eugenol synth references", Novel Discourse)Post 218431 (https://www.thevespiary.org/talk/index.php?topic=11362.msg21843100#msg21843100)
(PolytheneSam: "Re: ArOR, Alternatives to dimethyl sulfate", Novel Discourse)Post 221040 (https://www.thevespiary.org/talk/index.php?topic=11362.msg22104000#msg22104000)
(PolytheneSam: "Re: ArOR, Alternatives to dimethyl sulfate", Novel Discourse)Post 330874 (https://www.thevespiary.org/talk/index.php?topic=7674.msg33087400#msg33087400)
(Antoncho: "A very (IMHO) curious idea", Chemistry Discourse)Post 330714 (https://www.thevespiary.org/talk/index.php?topic=7674.msg33071400#msg33071400)
(Antoncho: "A patented improvement", Chemistry Discourse)Post 348592 (https://www.thevespiary.org/talk/index.php?topic=7674.msg34859200#msg34859200)
(Antoncho: "Methyl iodide methylation of 2-OH-5-MeO-BA.", Chemistry Discourse)Post 314724 (missing)
(Rhodium: "I rather methylate with Me2SO4 than MeI", General Discourse)Post 51160 (https://www.thevespiary.org/talk/index.php?topic=7607.msg5116000#msg5116000)
(obituary: "MeI methods", Chemistry Discourse)Post 299818 (https://www.thevespiary.org/talk/index.php?topic=7607.msg29981800#msg29981800)
(foxy2: "MeI and alkyl iodide synthesis", Chemistry Discourse)Post 301629 (https://www.thevespiary.org/talk/index.php?topic=7607.msg30162900#msg30162900)
(Antoncho: "Two tried-and-true ways to make MeI !", Chemistry Discourse)Post 331620 (https://www.thevespiary.org/talk/index.php?topic=7607.msg33162000#msg33162000)
(Antoncho: "Another trial.", Chemistry Discourse)Post 216461 (https://www.thevespiary.org/talk/index.php?topic=7501.msg21646100#msg21646100)
(foxy2: "Ethyl hydrogen sulfate", Chemistry Discourse)Post 190955 (https://www.thevespiary.org/talk/index.php?topic=7400.msg19095500#msg19095500)
(Antoncho: "CH3-C6H5SO2*CH3O - an OTC methylating agent?", Chemistry Discourse)Post 280978 (https://www.thevespiary.org/talk/index.php?topic=6387.msg28097800#msg28097800)
(Chromic: "Re: Tma from Tmma", Chemistry Discourse)Post 329531 (https://www.thevespiary.org/talk/index.php?topic=9131.msg32953100#msg32953100)
(Rhodium: "Aha, that's the key! You are supposed to take ...", Methods Discourse)SWIM had after the first trial hoped this drug was "the holy grail" he'd been looking for, a psychedelic that didn't bring too much disturbing stimulation, but made it easier to relax. Unfortunately it appears to be just as stimulating as most other related compounds
Have you thought about isolation of the R-isomere ? The S seems likely to be responsible for most of the body-load. Maybe R-DOM a step closer to the holy grail of psychedelics, see PIHKAL entry.
--psyloxy--
Beilstein Crossfire - DOM (racemat) (https://www.thevespiary.org/rhodium/Rhodium/chemistry/articles/beilstein/dom/dom.html)
(https://www.thevespiary.org/rhodium/Rhodium/chemistry/articles/beilstein/dom/dom.html)Beilstein Crossfire - DOM (R-isomer) (https://www.thevespiary.org/rhodium/Rhodium/chemistry/articles/beilstein/dom/r-dom.html)
(https://www.thevespiary.org/rhodium/Rhodium/chemistry/articles/beilstein/dom/r-dom.html)Beilstein Crossfire - DOM (S-isomer) (https://www.thevespiary.org/rhodium/Rhodium/chemistry/articles/beilstein/dom/s-dom.html)
(https://www.thevespiary.org/rhodium/Rhodium/chemistry/articles/beilstein/dom/s-dom.html)J. Med. Chem. 17(10), 1100-1111 (1974) (https://www.thevespiary.org/rhodium/Rhodium/pdf/sar.psychotomimetic.phenylalkylamines.pdf)
(https://www.thevespiary.org/rhodium/Rhodium/pdf/sar.psychotomimetic.phenylalkylamines.pdf)J. Med. Chem. 17(8), 877-882 (1974) (https://www.thevespiary.org/rhodium/Rhodium/pdf/dom.synthesis.resolution.pdf)
(https://www.thevespiary.org/rhodium/Rhodium/pdf/dom.synthesis.resolution.pdf)J. Org. Chem. 33(10), 3993-3995 (1968) (https://www.thevespiary.org/rhodium/Rhodium/pdf/tartanilic.resolving.acids.pdf)
(https://www.thevespiary.org/rhodium/Rhodium/pdf/tartanilic.resolving.acids.pdf)J. Med. Chem. 20, 414-421 (1977) (https://www.thevespiary.org/rhodium/Rhodium/pdf/dom.deuterio-synth.pdf)
(https://www.thevespiary.org/rhodium/Rhodium/pdf/dom.deuterio-synth.pdf)J. Med. Chem. 24(3), 299-304 (1968) (https://www.thevespiary.org/rhodium/Rhodium/pdf/n-hydroxy-dom.isomers.pdf)
(https://www.thevespiary.org/rhodium/Rhodium/pdf/n-hydroxy-dom.isomers.pdf)J. Med. Chem. 16(5), 480-483 (1973) (https://www.thevespiary.org/rhodium/Rhodium/pdf/nichols/nichols-asymmetric-amphetamines.pdf)
(https://www.thevespiary.org/rhodium/Rhodium/pdf/nichols/nichols-asymmetric-amphetamines.pdf)Patent US4000197 (http://l2.espacenet.com/dips/viewer?PN=US4000197&CY=gb&LG=en&DB=EPD)