Props to Wareami sharring info on Laquer Thinner in a PM.
Just now slowin down after awaking from a twisted dream.
This post shared as a template or spring board for yet more atacks for the gaacks.
Bare bone steps;
a)grind
b)Alc pull/filter
c)reduce vol
d)precip in LT (Laquer Thinner)
e)filter/rinse
Ok let the scoffing begin! SWIW found swiw's self with no acetone, a small bit of denatured, small bit of xylene, no drying agents (salt, mag-sulf). And way beyond unwilling to venture out for ANYTHING. Swiw's tweak melon was sure a procedure with what was availible existed and would hear of nothing more. Originally had in mind to xtract np from the LT to use on a A/B with ISO/Denat. Ya right! Would aparnetly rather climb a greased pole rather than take a set of steps to get upstairs too! Remembering Wareami's PM saying to make use of a mistaken purchase of LT rather than acetone and that LT in combo removes oranges and such, will let him share his findings. Don't want to possibly spoil his next writeup. The can says contains Acetone, Alc's,Ketones,Esters,Glycols,Pet- Distilates,etc. Swiw decided to give it a go as a premixed solvent like mixing NP and Alc to precipitate.
SO;
a) 8 box generic 120's ground in blender 90sec
b) aprox 42oz ISO & +/- 2oz Denat added w/stirring
c) Heated in micro more stiring (no boil)
d) Suction filter 2 times first 2ply charmin
plug topped with cotton plug lightly!-packed and
topped with 2 cotton disk pads. 2nd filtering
w/4plys plug packed tight cotton pad on top. When
all alc had been decanted on first filtering,
the GUPs n all were poured int the fliter and
and rinsed w/more ISO then left over sucction
filter. THen GUPs were put in ziplock just in
case. (C.Y.A.)
e) Reduce mix down to aprox 6 fluid oz. Want to
keep the denaturants free flowin and shift the
soulubility of psuedo down. Tone seems to
act as and open invite for psuedo to disolve with
orange present unless used in large amounts
quickly only to reduce loss not stop it.
f) In a tall caraffe/64oz+ beaker add LT (Laquer
Thinner) Boil out tone/alkies in micro Swiw
added about 20 oz to the reduced 6oz mix. Mix
began turning yellow as volume decreased. Micro
was intermitent with hand swirling to release
built up energy, not to fond of bumping! Mix
will reach a point where it sounds like
sizzling bacon. Remove from micro and swirl.
POW!, instant oatmeal. It needs to remain just
soupy enough to flow. Suction filter through
nonpacked cotton. SWIW poured the filtered fluid
back through to catch some of the precipitate
forming inside filt flask.Try not to let the
pseudo dry out before rinsing with the xylene.
Then SWIW let sit and packed down filter cake
while suction dried. filter cakewas incredebly
clean.
Rinse w/xylene
Leave in filter under suction
Burn tested on glass and even stood up to slight over heating w/out discoloration. Some black left behind though...In hind sight is was prob more sulfates from galssware than anything. seing the result SWIW got greedy and went for the mix in the rinse slop. BAD IDEA!!! (Bastard slugyfed)The first filter cake weighed in at 19.36g after drying out in the oven til bone dry. This was thankfully split into two piles as swiw forgot the bastard collection in the filter-funnel. One part from the clean cake was comined with fresh LT to do a test reboil so as to better gauge the disolving props of the LT on pseudo and as next step for further cleaning. Well like an idiot, the precip from this step got combined with the final dirty collection of the bastard stuff still in the funnel. SWIW did note that the second cleaning wasted pseudo. The Leverage here comes from the mostly dry ISO, (Denat, will try w/out it next), and the mix of the LT holding on to the denaturants with just enough acetone present in the LT to allow the Gaack to start it's thing, but it can't quite get a grip then it is rinsed away with a little xylene. The Still clean and dry half of the first pull was run in a semiwet PIE that lost it's lusteraround hour 5 and was worked up with a shot of TCE and a splash of jap before a final xylene rinse. Filtered again. Then based fisrt w/NaCO3 then small aditions of NaOH. Pulled 3x xylene (yellow tint remained even after boiling) rinsed 1x h20 and 1x brine solution (yes brokedown and went to store!) split the combined pulls part 1 gassed beautifly via hcl/CaCl the 2nd portiion titrated with a hint of yellow-to-red-to-green coloring of np. Titrated product was clean but not as clean as the gassed. After drying, gassed product left no trace on glass even when scortched to flamable stage. Poof! Titrated collection needed 2xrecryst to reach this point, however after a 3rd rextl from water was more potent. (duh!) Back to the Bastard tainted psuedo. Added to a portion of ISO and repeated begining precip steps. Every time step was performed the solutionbecame more viscous and a deeper shade of yellow to orange. The amont of psuedo seemed to drop only a little. After a PIE Orange Gacck proudly devoured the results at the end.
In conclusion, SWIW isn't sure if the orange was defeated in the begining or removed pre-basing at the end. Control group splips the mind in such excitement. What stood out in SWIW's mind was the purity of the pseudo in such a short time with high yeilds. Being a pessimist swiw opted to try and clean it up more thinking the high yeild was due to a trojan foe. Had SWIW not of TCE the end PIE solution swiw would have a better view. With the second pie producing such a high amount of orange SWIW is left to ponder the steps, and without accurate notes and an ongoing notation of even the littlest variations, well!
So this is the addition to swiws recollections of dreams that will be fine tuned and hopefully result in 3 possible solutions. Oh for Fuck Sake forgot to talk about the LT that had been prewashed with brine 3 times...later this is way long enough! out!
Oh ya Pie results: 1st 8.00 in 6.12 out
2nd 8.00 in 3.60 out