https://www.thevespiary.org/rhodium/Rhodium/chemistry/wacker.benzo-meoh.html (https://www.thevespiary.org/rhodium/Rhodium/chemistry/wacker.benzo-meoh.html)
Try that one. It's easy to read and works great.
If your pump pulls safrole over at 170, your ketone should come over at around 195. That's kinda high, but it should work ok.the washes don't have anything to do with the bp of your ketone, your pump does.
We'll soon find out if I'm a chemist or not!
"benzoquinone and CuCl both work to get the PdCl2 back to a +2 state", well PdCl2 is in a +2 state, the Pd(0) that is formed as part of the catalytic cycle, must be returned to the +2, so it can continue participating in the reaction. If i said the wrong thing in my PM that was because i was in a hurry and thats why i didn't post, but i didn't save a copy of my PM to OB1 so i don't know.
Got democracy? http://www.dhushara.com/book/multinet/democ/wed.htm (http://www.dhushara.com/book/multinet/democ/wed.htm)