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Post 428410
I think the top layer is the water and the bottom is the naptha? Which one should I use?
Wrong guess. If you want to "use" the naptha by titrating it, use the layer on top. The one that smells like naptha. (You did use hot naptha, didn't you?) Wash it the way suggested in the writeup Geezmeister pointed you to, then titrate it as he describes. But don't throw anything away just yet.