https://www.thevespiary.org/rhodium/Rhodium/chemistry/dob.html (https://www.thevespiary.org/rhodium/Rhodium/chemistry/dob.html)
https://www.thevespiary.org/rhodium/Rhodium/chemistry/nitrostyrene.nabh4.reduction.html (https://www.thevespiary.org/rhodium/Rhodium/chemistry/nitrostyrene.nabh4.reduction.html)
- the use of MeOH is not reccommended as it decomposes the NaBH4 too fast. I will add a note about that to the procedure written by Dr Gonzo.Post 301717 (https://www.thevespiary.org/talk/index.php?topic=7292.msg30171700#msg30171700)
(Antoncho: "2,5-diMeO-phenylnitropropene - the "cold" way.", Chemistry Discourse)