Bull.Soc.Chim.Fr., 39,4.1926;316Je ne parelé pas francaise ... but: Ph-SO
3Na + HSO
3Cl
__> Ph-SO
2Cl in 65% - TsOH
__> TsCl, same procedure, same yield.
J.Gen.Chem.USSR, 52,2.1982;341-343non too informative article, but yields are given when only 1.2 equiv. of HSO
3Cl are used. Actual procedure is in a russian ref.
Chem.Ber., 12.1879;1849-1850An old German article, only 50% yield. Rests here so nobody thinks there's better methods out there then presented in the patents above.
Just in case you didn't notice:
Post 514474
(psyloxy: "chlorosulphonic acid", Chemistry Discourse)--
psyloxy--