swig decided to post this dream as it was one of the best dreams he had in a while. Hes been passing sometime with lower yields, more because he was trying new stuff to modify the method he was applying before. So as u might guess lots of new changes and sometimes repeating stuff as he initially started but now with a better technique and understanding.
Ok i will try to underline here the major improve factors.
1- PFed -
Ok after several shit trying to follow what all are doing here he decided that to much shit was done but the yields were suffering or to expensive coz lots of solvents involved.
method as follow:
1-entire pills into the glass container. at least 60 pills at the same time.
2-using allways the some solvent used on previous pseudo washings. this solvent is in reality 2 solventes.
They are (writting here exactly what one can read in the container regarding english language):
-Turpentine (CAS nº 8006-64-2)
-White Spirit (CAS nº 64742-88-7)
boiling in microwave. 1 minute max power. rest 15 seconds. do this more or less till its boiling. Let it really boil. no problem. Im saying this coz in the beginning SWIG was kinda afraid of this kind of boils. There isnt such problem but plz beware not to caramelize it. do a good amount of boil but pay attention.
-decant this and PLZ keep it for reuse. Add acetone to clean this. decant and this acetone should be keeped so it can be used as the same way.
-Add 2 or 3 times the height with etanol (metanol seems equal thou its been while since i used methanol but i think its he same more centigram less centigram who really fukin cares?)
-put in freezer for some speed or let it stay at room temp undisturbed. covered preferably
allow 3 hours or less if u are going for a nano. u can extract the rest later after the first nano.
- filter using cotton balls on neck of funnel and a coffe filter.
- put liquid in a dish and take to the microwave. Put on max till boiling then use a lower setting,if by any chance some bee outhere as a identrical equip. to mine then do like this:
phase1 - 5:00 @ power 7
phase2 - 12:00 @ power 3
repeat this loop as necessary.
. how my microwave works???well my "potency" swithches if i dial in keypad like "potency button" then "number 7"...well this potency isnt really about giving like 850*0.70%=595 Watts...well it doesnt work nothing like this...you arent reducing the power but reducing the time which maximum power is working. For example this microwave wokrs like this (numbers arent accurate but give u what u need to understand):
full power - allways "on"...850 watts till u push off.
...
power 7 - 20 seconds full power+ 20 seconds no power cycle.
...
power 2 - 8 seconds on + 32 seconds off cycle and so on.
...
it has an addintional feature which is : I can sellect 2 heating phases at one time: for example 5 minutes @ full power then after these 5 minutes passes automatic to power 3 for 10 minutes for example. its a good micro mainly because it was 50 dol brand new....(i have to buy another...this was for food but im not much at house right now so...
)
This was only to say that u should boil alcool away but decresing the heat or u will end with burned shit which takes like 5 seconds to completly fuck the all batch.
-IODINE - After using the HCL+H2O2 method swig decides to revert to the H2SO4+Bleach like in rhodium site. changes are: 6.5% iodine per small bottle and 90 ml (3 uni.) instead of 100 ml.
Now SWIG has a doubt here...hes missing the maths here.
in rhodium site:
100 ml 5% iodine , 100 ml water, 5 ml H2SO4 96%, 24 ml bleach.
me:
90 ml 6.5% iodine, 90 ml water, 8-10 ml h2so4 98%, 24ml bleach
i didnt make any calcs. i use it. good yield but not 100%. can we get the 100%? what adjustments can be made to my quantities?
- RP comin from MB and was reused and maybe 15% of it was new.
REACTION:
material: gas stove, little but thick 60 ml bottle, 17 cm (didnt really paid much attention to meaures here) hose, ballon at one end and a sand bath with a identical little bottle with some water just to check when im close to the 100º C.
1.5 g PFED, 2.5 g I, 3.5 gr RP.
reaction took like 1 one hour to start. Since the fires in the flask SWIG is now scared with this type of yield killer so its better to take more time to start then burn the all shit.
A total of 10 drops of water were used (6 in the beggining 4 after 2 hours)
bettween ice bath and some heating the reaction as started and first phase has gone without any violence. it took some 25 minutes.
In this time water in the other bottle never boiled.
After heating was turned 25 minutes passed, 4 drops of water on and the cooking proceed for another 2 hours. so from putting reagents in the bottle and finishing it tooked 4 hours.
did the next procedure of filetring, washing and used Boiling nafta to extract. Tritate using HCL. the normal procedure and ended up with very glassy shit that burns leaving just a minor black point and that the totally the weight of 1 gr.
never yielded like this.
Important thing swig learned - 60 ml vessel is defenately the apropriate size (not 125 bor 250 that SWIG was using) and not having a fast 1st phaze (ice bath)
Peace and some ganza
