Hi,
i made a synthsis of meth like this
https://www.thevespiary.org/rhodium/Rhodium/chemistry/grignardimine.html
and at the before i recrystallized it get large crystals. I thought i did it. A friend of me show me some "speed" that he has bought and it smells after gymnastic-shoes and it tast very bitter. I recrystallized it i get get a white powder. 1st i did it in Isopropylalcohol and then in Xylol. But my meth smells after gasoline and it tast easily after salt. what did i wrong??? And the melting point was not the one of 175°C. It was higher than 350°C.
And at the End it is written that i have to satisfy the solution with dry HCL-Gas but how much must be injected??
And it is normally that I have a crystal-mash before i satisfy the solution with HCl-Gas???
And last but not least my last problem. I made it all like in the guidance but when i want to extract one phase i don´t see a Bar. I mean there is when i extract one phase e.g. EtO2 and Water ther is a Bar in the middle of the separating funnel but i don´t see any like this.
Can somebody help me please???
Thanxx...