The Vespiary

The Hive => Novel Discourse => Topic started by: TreSprit on November 26, 2002, 10:18:00 PM

Title: M from 3,4,5-Trimethoxyphenylacetonitrile
Post by: TreSprit on November 26, 2002, 10:18:00 PM

any good novel method of making M from this material. i dont have any vaacumapparatus. i would be working with 50g of subject material

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TreSprit
Chemical Generation

Title: At least get yourself an aspirator to use as a ...
Post by: Rhodium on November 26, 2002, 10:54:00 PM

At least get yourself an aspirator to use as a vacuum source, you will need it for distilling the freebase.

Reduction of phenylacetonitriles (benzyl cyanides) can be done with NaBH4/CoCl2, NaBH4/NiCl2, LiAlH4, CTH reduction with Pd/C and ammonium formate and many many other reagents. UTFSE! You can't have missed the mescaline section of my page, can you?