Author Topic: M from 3,4,5-Trimethoxyphenylacetonitrile  (Read 1481 times)

0 Members and 1 Guest are viewing this topic.

TreSprit

  • Guest
M from 3,4,5-Trimethoxyphenylacetonitrile
« on: November 26, 2002, 10:18:00 PM »
any good novel method of making M from this material. i dont have any vaacumapparatus. i would be working with 50g of subject material

TreSprit
Chemical Generation

Rhodium

  • Guest
At least get yourself an aspirator to use as a ...
« Reply #1 on: November 26, 2002, 10:54:00 PM »
At least get yourself an aspirator to use as a vacuum source, you will need it for distilling the freebase.

Reduction of phenylacetonitriles (benzyl cyanides) can be done with NaBH4/CoCl2, NaBH4/NiCl2, LiAlH4, CTH reduction with Pd/C and ammonium formate and many many other reagents. UTFSE! You can't have missed the mescaline section of my page, can you?