Author Topic: MDA with NaBH4 and am acetate review.  (Read 8543 times)

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scram

  • Guest
How much EDTA
« Reply #40 on: September 25, 2002, 08:48:00 AM »
Regarding EDTA: I could really use this information. What amount would be needed for ketone. Just a saturated solution? There are still too much copper compounds left in undistilled ketone even after 6 to 8 a/b washes.

Rhodium

  • Guest
Each molecule of EDTA complexes one copper atom.
« Reply #41 on: September 25, 2002, 12:20:00 PM »
Each molecule of EDTA complexes one copper atom. I don't know how much copper there is in your solution.

hCiLdOdUeDn

  • Guest
what about ammonia? Doesnt ammonia complex with ...
« Reply #42 on: September 25, 2002, 01:53:00 PM »
what about ammonia? Doesnt ammonia complex with copper ions also?

To bee or not to bee, that IS the question.

Rhodium

  • Guest
Yes, just not as strongly.
« Reply #43 on: September 25, 2002, 02:45:00 PM »
Yes, just not as strongly. Ammonia would react with MDP2P though.

Sunlight

  • Guest
CTH procedure
« Reply #44 on: September 27, 2002, 04:49:00 PM »
Just to remember you that the CTH reductive amination with ammnonium formate and Pd/C on MDP2P has shown to give high yields of MDA, check my post about it.