congradulations Dex and thanks for caring about civil liberties.
I suggest you read Post 428410 (https://www.thevespiary.org/talk/index.php?topic=8697.msg42841000#msg42841000)
(geezmeister: "The post-reaction workup: a cook's summary", Stimulants)
and Post 505807 (https://www.thevespiary.org/talk/index.php?topic=8569.msg50580700#msg50580700)
(wareami: "48hr mark....", Stimulants).
Wareami answered this for you last time through and the
Geez is phenominal from what I've read here.
Geez know's the facts and has taken the time to express
them in a way that is understandable, efficient
and thorough.
Your results, if this post is followed accurately, should
be optimized and of high quality.
Congradulations again and I am sure you will post results.
Look at Post 494033 (https://www.thevespiary.org/talk/index.php?topic=8664.msg49403300#msg49403300)
(Rhodium: "The condenser crystals are PH4I, not PI3!", Stimulants)
Let the reaction cool and settle. Rinse them down with dH2O. Work up; you're on the home straight!