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Author Topic: GBL Questions...Please Help a Gal...  (Read 1689 times)

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fastsally

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GBL Questions...Please Help a Gal...
« on: July 08, 2004, 12:06:00 AM »
Hello all :)  
I need some help converting GBL into THICK GHB.  I tried it a while ago and did something wrong.  I used baking soda instead of ACS NaOH and ended up with 2 distinct layers.  Top was fairly clear and the bottom was milky.  It's supposed to be totally clear right?PH stayed around 8 - 8.5. It's supposed to be totally clear right?  Any help or ideas of what I'm doing wrong would be appreciated.  Oh, the GBL is NOT ONCE REMOVED.  I get it from a chemical company the msds says 99% GBL.
thanks,
sally
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hypo

  • Guest
sorry, i lost my crystall ball
« Reply #1 on: July 08, 2004, 12:11:00 AM »
if you want people to help you, then tell them what you did!

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fastsally

  • Guest
Some more info. New problem...
« Reply #2 on: July 10, 2004, 08:02:00 PM »
Okay, Now I really feel like an idiot.  After taking a closer look at the label on my GBL I've found that it not only contains GBL but N-Methyl -2-pyrrolidone as well.  I guess this explains a lot of the trouble I've been having with converting to GHB.  Can anyone help me?  Can the N-Methyl... be removed or should I find a new GBL source.  I would really appreciate any help.
Thanks,
Sally
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Rhodium

  • Guest
Post 83268
« Reply #3 on: July 11, 2004, 03:07:00 AM »

Post 83268

(Rhodium: "Separation of NMP and Butyrolactone (GBL)", Chemicals & Equipment)

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