Hello Fellow bees,
Swim has been using TFSE for a loooong time now and has learned alot.
Swim wants to make sure he understand the washes in
BS synth correctly.
After 7 hours swim will flood solution with acidic water (50ml HCl+1.5L water)shake and let it settle.
Dump(throw out) out top layer.
Then swim will wash bottom layer with 100ml DCM.
Wash top layer again with 100ml DCM.
Combin2 2xDCM wash and organic layer. stir??
Wash DCM/organic layer with 150ml 10%NaOH.
Dump out top layer and wash bottom layer with another 10%NaOH.
Dump top layer keep bottom layer
Put in freezer or distill,
Is this correct?
Thankz !!
ps. Is swim supposed to flood with all 1.55L of acidic water or only a portion ??