Author Topic: Phenylpropanolamine Source?  (Read 2767 times)

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xbnmx

  • Guest
Phenylpropanolamine Source?
« on: February 01, 2004, 08:29:00 PM »
The only viable source of phenylpropanolamine I was aware of was otc pill extraction, but all of these drugs have vanished fromt he shelves and the only ones I am aware of which are still for sale are special pet medications which require a prescription.  Is anyone aware of another source or of a posible synthesis route?

silenziox

  • Guest
What's the wrong with you?
« Reply #1 on: February 01, 2004, 08:37:00 PM »
What's the wrong with you? Don't you ever take advantage of TFSE, altavista/google or rhodium.ws?

Benzaldehyde+nitroethane+triethylamine to the nitroethene,
then reducting to the alcohol with Zn/formic, for example.


Bandil

  • Guest
Link
« Reply #2 on: February 02, 2004, 01:20:00 AM »
Benzaldehyde+nitroethane+triethylamine to the nitroethene
To much THC there eh?  ;)  I think you meant :"to the nitroalcohol"

Follow

this

(https://www.thevespiary.org/rhodium/Rhodium/chemistry/para-fluoro-4-mar.html) procedure and omit the last two steps to get your PPA. Use regular benzaldehyde instead of the fluoroinated version of course!

Regards
Bandil