The cheapskate write-up is nowhere as simple as it reads. After swim's toying with batch sizes, parameters, cooling methods, and the all too famous billowing white solids that can't be vac filtered (without special fritted disks or what the fuck ever else one might use besides qualitative grade filter paper), the two of us can only conclude that we should have saved the ACS THF for lithium aluminum hydride reductions like for 2-cb.
Aqueous methods are wasted time. If i see pool shock again before i die it will be too soon.
I'd put a little more faith in that whole procedure if someone could give us a formal write-up INCLUDING A BIOASSAY of the final product. If I'm wrong about what I did, I'd surely welcome a correct path.
Cheapskate, I mean no disrespect. Your contribution in the OTC quaalude synth was, and still is, awesome.