Allrighty have comprehended the dir of the thread......um this bee uses um dexsulfate um pharmo ussually sticking to the thirty mg reaction per ussual, this he does um ussing no water ussing instead meoh tone and white gas he thinks there is something in this gas to mainly copper and some ammonia making this gas look bluish, other than this there may in fact be added to this whit gas some a largish amount of co it seems this also will turn to a bluish hue. Anyways ussing most dry salt mainly cacl the idea is to basicially issolate the amine from the garbage binders etc to create the cl ssalt if this even be possible. Now upon reading he dare not differ from the advice or recomendation only to say hoho is used in very small amounts not big ammounts rembering this is a small reaction 30mg in about four cup reaction vessel. thus anyways he starts to do a basic "CURE" prewashing the junk, then and this be done hot, accidently sometimes the other solvent is used on ocassion. Anyways the is rinsed in hot meoh then hot tone sometimes these are used rather together to keep the amine from going into the meoh, anyways the dex sulphate is supoprisingly insoluable in just about anything and alas a new easy water extraction is perfected more on that later.....anywas then hot gas is ussed to rinse, um all this is saved in threee bottles, and further use is sometimes used rectcled the dirt is removed by freezing the stuff a wax like shit comes out and also simply letting it sit then some crap sometimes falls out simply pouring of the top seem to clean it up[the solvent] anyways it is desicated dry crackling dry a few times, it never is done the same way twice
so there is a mixture of tone and meoh to this is seem to be added a bit of lye maybe a few grains mostly though threre is a goodly amount of cacl added throughout even durring washing steps, anyways it is heated up until it does in fact snow down from the np layer in nice snow flakes, then it is allowed to cool and slight swirling seem to lap up the good stuff into rocks, there is before this final stage, it the entire reaction is cooled before the final addation of a few grains of naoh, what happens in this prefinal stage is that the entire is gassed per foil and cacl and salt/muratic thus it the stuff is gasses and allowed to stand overnight, this is when the milky layer results it is semi solid looking milky and smeels different sweetish, this heavy solvent is "loaded" then anyways it is reheated up a bit of lye or most preferably I hate "lye" I prefer to use washing soda made from baking soda thankyou!
Anyways upon reheating the soup maybe adding a bit of fresh solvent, the stuff like laps up into the non polar layer the emmulsion clears the stuff the bottomerost layer mixxing compleatly the phases begin to become one solid phase except for a tiny film that being mostly salt on the bottom and a tiny film of oily looking stuff upon that on the bottom the rest basicially bubbles and compleatly mixed it is now that it is turned off removed from heat this is stirred by hand to....now swirling the entire it happens just like a commet smashing to earth, slam the stuff heavy stuff the clorosolvent hits heavy laden with salt first, as this heavy solvent hits the amine can be see popping out flating boyant upon the clorosolvent looking like popcorn, or wax like, yes it grows clumping together like a magnet attracts metal fillings, never the less the lower layer gets biger and bigger not turning milky cause it is hot still, ya add cacl untill it is saturated hot, maybe adding a bit of naoh to salt it out I think not shure, it is not a fussy procedure to figure out it will though take at minimium ten times to perfect to any degree of perdictiabality]
good luck!
Amethystium