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Author Topic: Distillation of 2,5-DMP2P at atmospheric pressure?  (Read 1873 times)

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Tezcatlipoca

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Distillation of 2,5-DMP2P at atmospheric pressure?
« on: August 13, 2002, 04:27:00 AM »
Can 2,5-DMP2P bee distilled at atmospheric pressure without damaging the molecule? TFSE only refers to atmospheric distillation of MDP2P; could find nothing about DMP2P.

Thanks in Advance,
Tezcatlipoca
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Osmium

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I wouldn't do it. At least use an aspirator ...
« Reply #1 on: August 13, 2002, 04:29:00 AM »
I wouldn't do it. At least use an aspirator vacuum.
I'm not fat just horizontally disproportionate.
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Mountain_Girl

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Maybe
« Reply #2 on: August 13, 2002, 06:01:00 AM »
Well, P2P can be distilled at atmospheric pressure so I have to wonder...what effect do those methoxies have...wouldn't be surprised if you could get away with it...but then I think Osmium has far more credibility than I so maybe his advice is the smarter move...
(and now I'm wondering if this post is of any use at all..)
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Rhodium

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The effect of those methoxies is a considerably ...
« Reply #3 on: September 02, 2002, 05:00:00 AM »
The effect of those methoxies is a considerably higher boiling point, as well as an inherent desire for the molecule to cyclise into a furan-type compound, if you have just a little bit of acidic or basic impurities in there.
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