Now we will distill the oil under reduced pressure and at a relatively high temperature. ... At full water pressure, the oil bath will need to reach 195 Celcius before the 2,5DMPEA will start to come over as clear, waterlike oil. Keep the temperature and pressure constant as the oil slowly drips over.
My question: Will distilling off the 2,5 DMPEA at 195° cause any decomposure of the product, and if so, are there any other viable alternatives. I don't see fractional freezing as practicle if it comes off at 195° under vacuum.
If this belongs in the Newbee forum, please relocate accordingly.
Thank you.
Carboxyl