The Vespiary

The Hive => Methods Discourse => Topic started by: del72 on August 16, 2003, 12:06:00 PM

Title: reaction times for regioselective halogenation?
Post by: del72 on August 16, 2003, 12:06:00 PM

My friend is going to be doing the regioselective iodination on 2CH using oxone and KI via this route on rhodiums site-

https://www.thevespiary.org/rhodium/Rhodium/chemistry/oxone.aromatic.iodination.html (https://www.thevespiary.org/rhodium/Rhodium/chemistry/oxone.aromatic.iodination.html)

.  The synthesis says that the the reaction was monitored using TLC until complete.  It is not  practical for my friend to monitor using TLC, so he was wondering if any bees who have carried out this reaction could suggest reaction times.  I have utfse with no luck so any help would be appreciated.

Title: UTFSE!
Post by: SpicyBrown on August 17, 2003, 05:28:00 AM

UTFSE for iodination, 2C-I and Barium.