Post 496227 (https://www.thevespiary.org/talk/index.php?topic=10009.msg49622700#msg49622700)
(lugh: "Adams' Articles", Newbee Forum)Post 484211 (https://www.thevespiary.org/talk/index.php?topic=13201.msg48421100#msg48421100)
(adroit_synth: "Mycelium Extraction", Tryptamine Chemistry) Tryptamine Chemistry adroit_synth 01-23-04 12:20Post 482134 (https://www.thevespiary.org/talk/index.php?topic=13201.msg48213400#msg48213400)
(adroit_synth: "Psilocybin Production", Tryptamine Chemistry) ...off and it is allowed to cool in the oven. Each jar should yield 50-100g of wet mycelium which is about 90% water, for a dry yield of 5-10g of crumbly material. Extraction The dried mycelial material is crumbled and pulverised, nd each 100mg of this is combined in a flask with 10ml of absolute methanol. The flask is placed in a hot water bath for four hours. The liquids are collected and saved. The slurry (the mushPost 460964 (missing)
(GC_MS: "Psylocybin/psilocin extraction the Czech way", Tryptamine Chemistry) Tryptamine Chemistry GC_MS 09-25-03 06:13Post 450823 (missing)
(Aurelius: "Cland Drug Labs J. For Sci 15,1, 51-64 (1970)", General Discourse) General Discourse Aurelius 07-31-03 01:01Post 449484 (https://www.thevespiary.org/talk/index.php?topic=13107.msg44948400#msg44948400)
(urushibara: "psilocybin precipitate *would* be quite pure imo", Tryptamine Chemistry) Tryptamine Chemistry urushibara 07-24-03 04:56Post 397222 (https://www.thevespiary.org/talk/index.php?topic=13107.msg39722200#msg39722200)
(Yachaj: "Psilocybine crystallization for beginners", Tryptamine Chemistry) ..., there's all sorts of junk (the major crap in there is urea, you can smell it when it's evaporated down), but the use of ethanol is selective for precipitating the psilocybin. most everything that was named is much more soluble in ethanol than psilocybin. on another note, rhodium just posted on another thread about a method of doing an acid/base extraction on psil...Post 449383 (https://www.thevespiary.org/talk/index.php?topic=12923.msg44938300#msg44938300)
(Rhodium: "Mushroom Aqueous-Organic Psilocin Extraction", Tryptamine Chemistry) Tryptamine Chemistry Rhodium 07-23-03 22:00Post 448065 (https://www.thevespiary.org/talk/index.php?topic=12923.msg44806500#msg44806500)
(uneasyone: "tryptamine cubensis---->psilocin hcl extraction", Tryptamine Chemistry) An Aqueous-Organic Extraction Method for the Isolation and Identification of Psilocin from Hallucinogenic Mushrooms Casale, J. F. Journal of Forensic Sciences, Vol. 30, No. 1, pp. 247-250 (1985) (https://www.thevespiary.org/rhodium/Rhodium/chemistry/psilocin.extraction.html (https://www.thevespiary.org/rhodium/Rhodium/chemistry/psilocin.extraction.html)
) Abstract A simple a...Post 449051 (https://www.thevespiary.org/talk/index.php?topic=13107.msg44905100#msg44905100)
(Yachaj: "Lilienthal wrote: "your product is a...", Tryptamine Chemistry) Tryptamine Chemistry Yachaj 07-22-03 08:32Post 397222 (https://www.thevespiary.org/talk/index.php?topic=13107.msg39722200#msg39722200)
(Yachaj: "Psilocybine crystallization for beginners", Tryptamine Chemistry) ...in ethanol" True. But the undesired components do not interfere enough with the solubility of the major psychoactive component (PSOP) to make the standardized extract unreliable. But hey - look at this. It is about the use of 4-DMCA instead of 4-DMBA as main ingredient in Ehrlich's reagent. 4-DMCA is OTC and most likely useful as indicator when a simple piece of typing paper is used as TLC surface. From the paper then all different components can be sepa...Post 448779 (https://www.thevespiary.org/talk/index.php?topic=12923.msg44877900#msg44877900)
(urushibara: "dephosphorylation", Tryptamine Chemistry) Tryptamine Chemistry urushibara 07-21-03 03:39Post 448065 (https://www.thevespiary.org/talk/index.php?topic=12923.msg44806500#msg44806500)
(uneasyone: "tryptamine cubensis---->psilocin hcl extraction", Tryptamine Chemistry) ...nset is to take it on an empty stomach. this was with dried cubensis. what about deliberately providing the fungi with adequate phosphorous to increase the ratio of psilocybin that is formed? psilocybin is easier to extract, just soak/simmer and filter/freeze and there it is. it could be snuffed I suppose, I don't see why that wouldn't work. maybe dissolved in water in a nasal sprayer.