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Author Topic: Please help! Need help with steam distillation of  (Read 1726 times)

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slick14

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Please help! Need help with steam distillation of
« on: July 02, 2003, 05:42:00 PM »
Someone please help swim has searched tfse and cannot find the temp at which the MDMA fb comes over using steam distillation someone please help.  Also any special concerns in the above procedure thanks for any help.

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Barium

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?
« Reply #1 on: July 02, 2003, 05:49:00 PM »
Steam distillation takes place at the boiling point of water

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smutboy420

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you can't distill mdma freebase with steam
« Reply #2 on: July 02, 2003, 06:15:00 PM »
nope anin't going to happen. you need to vac.distill it. and it should come over at 10 deg.C higher then your ketone came over at. so if you got ketone at say 144c then your fb will come over at 154c using the same vac as you used for ketone.
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Rhodium

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Steam distillation not suitable
« Reply #3 on: July 14, 2003, 12:55:00 AM »
Give up, and vacuum distill. Even when distilling MDP2P, you have to distill 100mL of water for every mL of MDP2P coming over.
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