Instead of using the messy preparation from Pihkal requiring solvent extraction to synthesize the 2,5-dimethoxynitropropene, instead use the procedure at https://www.thevespiary.org/rhodium/Rhodium/chemistry/edda.html (https://www.thevespiary.org/rhodium/Rhodium/chemistry/edda.html)
which gives an equal yield, higher purity, and also produces the 2,5-dimethoxynitropropene in crystalline form directly.
If you still feel you want to use the Pihkal procedure, you can substitute the chloroform with dichloromethane.