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Electrochemical Reduction of Nitrostyrenes

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Osmium:
I had one for less than 100$, complete with 2 digital meters for current and voltage, regulatable between 0-3A and 0-30V, so that price is possible.

Unobtainium:
I wish I knew where you bought your power supplies from. My 0-18v/0-3A variable cost over $300.




Please Email all complaints of my performance to hive@lycaeum.org

Osmium:
www.conrad.com is one of the best sources for electronic equipment I know of. At least for Euro bees.

That power supply was bought at a local shop. No way I will tell you bees where I live  ;)

Rhodium:
The article mentioned and partially translated in Post 47461 (uemura: "Electrochemical Reduction of Nitrostyrenes", Novel Discourse)

Über -Phenyl-äthylamine. III. Neue Darstellung von Mescalin
K. H. Slotta & G. Szyszka
J. Prakt. Chem. 137, 339-350 (1933) (https://www.thevespiary.org/rhodium/Rhodium/pdf/mescaline.slotta-szyszka.pdf)

Rhodium:
Here are the other parts in the same series:

Über -Phenyl-äthylamine. I. Mescalin und Mescalin-ähnliche Substanzen.
K. H. Slotta & H. Heller
Chem. Ber. 63, 3029-3044 (1930) (https://www.thevespiary.org/rhodium/Rhodium/pdf/mescaline.slotta-heller.pdf)

Über -Phenyl-äthylamine. II. Eine Neue Tyramin-Synthese
K. H. Slotta & W. Altner, Chem. Ber. 64, 1510-1520 (1931)
Posted in Post 477747 (lugh: "Tyramine Preparations", Chemicals & Equipment)

Über -Phenyl-äthylamine. IV. Darstellung von -[Amino-phenyl]-äthylaminen.
K. H. Slotta & G. Szyszka
Chem. Ber. 68, 184-192 (1935) (https://www.thevespiary.org/rhodium/Rhodium/pdf/pea-4.slotta-szyszka.pdf)

...and here the poor chemists are flamed by a colleague for saying in Part 3 above that their synthesis of mescaline was better than his...  ::)

Synthese des Mescalins (Entgegnung auf die "Berichtigung" von K.H. Slotta und G. Szyszka)
Georg Hahn
Chem. Ber. 67, 1210-1211 (1934) (https://www.thevespiary.org/rhodium/Rhodium/pdf/mescaline-flame.pdf)

Here are his own contributions to mescaline chemistry - you can judge yourself:

Über -[Oxy-phenyl]-äthylamine und Ihre Umwandlungen. I. Synthese des Mescalins.
Georg Hahn und H. Wassmuth
Chem. Ber. 67, 696-708 (1934) (https://www.thevespiary.org/rhodium/Rhodium/pdf/mescaline-hahn.pdf)
____ ___ __ _

Über -[Oxy-phenyl]-äthylamine und Ihre Umwandlungen. II.
Synthese weiterer Amine und der entsprechenden [Oxy-phenyl]-essigsäuren aus naürlichen Allylverbindungen.
Georg Hahn und Otto Schales
Chem. Ber. 67, 1486-1493 (1934) (https://www.thevespiary.org/rhodium/Rhodium/pdf/allyl2paa2pea.pdf)

And finally, some further elaborations on phenethylamine syntheses by his collaborator on the second paper:

Über -Substituierte Äthylamine. I.
Ein einfaches Verfahren zur Darstellung von -Phenyl-äthylaminen aus -Nitro-styrolen.
Otto Schales
Chem. Ber. 68, 1579-1581 (1935) (https://www.thevespiary.org/rhodium/Rhodium/pdf/schales.ns2pea.pdf)
____ ___ __ _

Über -Substituierte Äthylamine. II. Die katalytische Hydrierung von Oximen.
Otto Schales
Chem. Ber. 68, 1943-1945 (1935) (https://www.thevespiary.org/rhodium/Rhodium/pdf/schales.oxime2pea.pdf)

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