https://www.thevespiary.org/rhodium/Rhodium/chemistry/safrole.distillation.html (https://www.thevespiary.org/rhodium/Rhodium/chemistry/safrole.distillation.html)
http://www.biggreenegg.com/boilingPoint.htm (http://www.biggreenegg.com/boilingPoint.htm)
to calculate the temperature your water should be boiling at based on your barometric pressure.Post 278285 (https://www.thevespiary.org/talk/index.php?topic=7071.msg27828500#msg27828500)
(RoundBottom: "Re: vacuum refluxing", Chemistry Discourse), it's not rocket science, people.Bull.Soc.Chim.Fr.; 1964; 1892. (https://www.thevespiary.org/rhodium/Rhodium/pdf/benzodioxole.deriviatives.pdf)
(https://www.thevespiary.org/rhodium/Rhodium/pdf/benzodioxole.deriviatives.pdf)Post 385717 (https://www.thevespiary.org/talk/index.php?topic=12142.msg38571700#msg38571700)
(Rhodium: "Isosafrole via Wittig Olefination of Piperonal", Novel Discourse)Post 431447 (https://www.thevespiary.org/talk/index.php?topic=8953.msg43144700#msg43144700)
(FriendlyFinger: "Safrole Isomerising methods", Methods Discourse) Safrole Isomerization (KOH/n-BuOH, 3h @ RT, 98% trans-isosafrole)Post 431447 (https://www.thevespiary.org/talk/index.php?topic=8953.msg43144700#msg43144700)
(FriendlyFinger: "Safrole Isomerising methods", Methods Discourse) Safrole Isomerization (KOH/n-BuOH, 3h @ reflux, 95% yield)