Author Topic: Stability of nitrostyrenes?  (Read 674 times)

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KidCurry

  • Guest
Stability of nitrostyrenes?
« on: April 28, 2004, 11:31:00 AM »
If someone would make for example 3,4,5-TMNS, is it stable enough to be stored in a airtight container under roomtemp for 3-4 weeks? (Sorry, but search-function is not working as we all know. :P)

Bandil

  • Guest
If purity is OK
« Reply #1 on: April 28, 2004, 11:39:00 AM »
If you have recrystallized and purified your nitrostyrene properly, it is no problem storing it for longer periods of time.


KidCurry

  • Guest
Thank you very much. Would oneĀ ...
« Reply #2 on: April 28, 2004, 11:49:00 AM »
Thank you very much.
Would one recrystallisation from methanol be enough? Or should someone do it twice? The method of preparation would be condensation of 3,4,5-TMBA with nitromethane (in excess, as solvent too) and ammonium acetate? If my memory serves me well I think this method will produce a not so very clean product?