if one were to theoreticaly use the formula and technique exactly as descrtibed by Krz post at Rhodium, she might get no results at all, as snakebite. After extensive use of TFSE, it seems the details of that post were removed by the author.
Other posts indicate shaking heavily may help o2 absorbtion, while CuCl rahter than the dihydrate of Cucl2 is the answer. Then there is the DMSO suggestion.
I cannot seem to find a complete post of any success with the o2 wacker, sans PBQ, except for the shake it and leave it under the bed for 18 hours listing.
If heating will drive yields towrds P1P,is there any way to salvage snakebites unreacted mix? Will shaking while at 35-40 psi create the uptake after that same rxn mix has seen no activity but remained under o2 press for 48 hours?
It would be a damn shame to waste so much of so many critical reactants without trying a save. Any follow us advice would no doubt be greatfully appreciated by all at such a sticking point.