sorry to be posting this spam, but i need to find a post made a few months back (yes have UTFSE for two hours now, pas de luck)
it was the basic vacuum isomerisation technique minus the vacuum, no solvent, i forget who posted it, but they had just tested a batch of safrole w/ KOH on a waterbath overnight.
the thing i remember most about it was somebee said, "my vacuum will sleep alot easier now" or something such
I need a low temp iso technique for a very special allybenzene, cannot risk polymerization and haven't got any PTC to hand, please help!
anybee know the post i mean, or the technique? i remeber thinking it was ALOT of KOH at the time but . . . i guess my brain is charred
"All those memories lost like rain..."