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Author Topic: New use for the leftovers from sas distilling.
gyrogearloose [Image] posted 01-09-99 04:27 AM
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Last post here for me.
I know someone will spit on this but here goes anyway.
In the recent past I discovered that if you saver the
leftovers from distillation of sassafras you can use it
to distill the ketone without burnt stuff leftover, it
works better than cooking oil or peanut oil(tried both)
you can use it over and over and over.
Well now shit on it as fast as you can.
Bye.
ChemHack [Image] posted 01-09-99 09:26 PM
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When distilling safrole I am often left with a thick
darkBrownBlackish gunk. Is this the stuff you are
talking about?
Sometimes during safrole distillation some of it gets
charred onto the boiling flask. If you re-use the
leftovers in this way will the charring also happen or
does it only happen the first time when doing the
safrole? (ie all that can char does char)
I take it that it has a bp that is higher than the
ketone as well....
I suppose you could also use it if you were gonna
distill the freebase amine at the end...
Whadda ya think?
ChemHack [Image] posted 01-09-99 09:28 PM
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PS: I hope you don't think that I am shitting on your
idea. I like it.
gyrogearloose [Image] posted 01-11-99 04:35 AM
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Nah, I don't think you are shitting on it, as for me
When I distill it I don't go quite that far to end up
with dark brown stuff I stop as soon as the temp in the
top of vageraux colmn gets higher than safrole temp,
thus I am left with a little darl yellow stuff each
time and I add it to a supply of it and then use it to
distill ketone over without charring. It does boil
higher, all those things that don't come over fast.
beats cooking oil or cottenseed oil for me anyway. I
even use it to distill over iso sometimes same
results......
Standard disclaimer here#####
you know don't try this at home, it may be against the
Law, you could get hurt, you don't have a note from
your Mom, only ment to entertain. or amuse.
ChemHack [Image] posted 01-11-99 01:42 PM
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I doubt that this would work very well for the oil that
I currently use. The reason is that there does not seem
to be a clear "break" in the boiling point.
For example: At atmospheric pressure it begins to boil
about 232C but the temp continues to rise as clear
safrole comes over. The contents of the distilling
flask get darker and darker and by the time it hits
245C only a black oil remains. I imagine that if
heating was continued that the temp would continue to
slowly rise as the shit got thicker and thicker and
finally charred.
So, even if I leave that "other" stuff behind when
distilling safrole, it will likely come over anyway
when distilling higher boiling oils like iso-saf or
ketone.
I really like your idea, I just don't think it would
work very well for me any my particular oil....
gyrogearloose [Image] posted 01-15-99 02:57 AM
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See me for good oil......
Stonium [Image] posted 01-15-99 07:20 AM
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gyrogearloose: You said: "See me for good oil."
OK, how do I that? email: stonium@hotmail.com
Muchas Gracias,
Stonium
Methyl Man [Image] posted 01-15-99 05:38 PM
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Mr. Gyrogearloose: would you mind imparting that info
to me as well?
b_marapuna@hotmail.com (no, it's not my real name!)
thanx
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