The Vespiary

The Hive => Methods Discourse => Topic started by: nitrous351 on June 19, 2003, 06:21:00 PM

Title: Column length for MM Hg/Al
Post by: nitrous351 on June 19, 2003, 06:21:00 PM

SWIM wants to do the MM Hg/Al reaction in a 2Litre, 2 neck flat bottom flask. Is a 200mm condenser enough to contain the reflux? Would it be better to stack the condenser on top of a vigreux column? How are the smells for this reaction? THanks Peace

Title: Unsure
Post by: Aurelius on June 19, 2003, 08:43:00 PM

Anytime that you are unsure and have the available materials/glassware, it is a good idea to add another bit of length.  Put a short or medium length vigreaux on there and then the condensor, it won't hurt*, but it may help.

*https://www.thevespiary.org/rhodium/Rhodium/chemistry/alhg-meno2.html
  This gives additional notes on the factors can influence the reaction.  So, yes it may be affected, but it shouldn't be by much.

Title: Or if containing a runaway reaction is the concern
Post by: runne on June 22, 2003, 05:07:00 PM

Or if containing a runaway reaction is the concern you could add a length of clear vinyl tubing or other such tubing to contain the possible Al/Hg Volcano.