The Vespiary

The Hive => Newbee Forum => Topic started by: edgy on May 02, 2004, 09:26:00 PM

Title: p2p please
Post by: edgy on May 02, 2004, 09:26:00 PM

i have successfully used benzaldehyde and l alanine to make ppa. could someone please give me a detailed procedure whereby i could produce p2p. someone mentioned ppa plus aluminium chloride and hcl to make p2p. could this be outlined in lay terms for a novice? also can i produce aluminium chloride? thankyou for your due consideration.

Title: Heres the AlCl3 info.
Post by: ApprenticeCook on May 03, 2004, 05:07:00 AM

Heres the AlCl₃ info.

https://www.thevespiary.org/rhodium/Rhodium/chemistry/aluminumchloride.html (https://www.thevespiary.org/rhodium/Rhodium/chemistry/aluminumchloride.html)

-AC

Title: PPA -> P2P
Post by: Rhodium on May 03, 2004, 06:54:00 AM

PPA -> P2P (https://www.thevespiary.org/rhodium/Rhodium/chemistry/phenylacetone.html#ephedrine)

(https://www.thevespiary.org/rhodium/Rhodium/chemistry/phenylacetone.html#ephedrine)

Title: You could make P2P...
Post by: ning on May 03, 2004, 04:34:00 PM

...but why not bee classy and make 4-methylaminorex instead? With that PPA, you are so, so close....

Title: 4-mar troubles
Post by: edgy on May 03, 2004, 08:10:00 PM

firslty thankyou for your replies. in answer to ning,  the 4-mar presented swim with troubles last time. mainly with trying to extract the precipitate after mixing ppa with product of sodium carbonate and urea , (which smelled alot to make.)
i have noticed the thread has progressed and will read it but i would appreciate any knowledge you could impart.

Title: try...
Post by: chilly_willy on May 07, 2004, 02:26:00 AM

If you have the benzaldehyde...try this:

Post 392078 (missing)

(Aurelius: "P2P synth", Methods Discourse).  It works!  With practice the yields go UP....