dropping the sulfuric acid through a tube to the bottom of the vessel.
Bad idea. This will clog.
Using a KIPP principle apparatus and an excess of NaCl could work.
ADDON:
Good news! I found a procedure describing the production of chlorine by using NaCl/H2SO4 onto MnO2 instead of the ususal HCl onto MnO2. It is told this being advantageous for more chlorine being produced and for the H2SO4 scavenging H2O from the reaction.
So there is little doubt that this will work just fine with TCCA. The only question left is if not TCCA is a too expensive material for this task - MnO2 maybe not everywhere available with ease but if MnO2 isnt, FeO2 is (for coloring cement) and I believe this will work as substitute for MnO2.
Reference:
- Manual of Inorganic Chemistry, Charles W. Eliot and Frank H. Storer, 1876, page 106.
Post 100482 (missing)
(Atomicdog: "Chlorine gas generation", Chemistry Discourse) ;)Post 468552 (https://www.thevespiary.org/talk/index.php?topic=7197.msg46855200#msg46855200)
(politoxicomania: "Gas SWIM needs", Chemistry Discourse)