The Hive > Tryptamine Chemistry
AMT in the MW oven
yellium:
Also, indicate _where_ you've drilled the hole (and give its size); plus sizes of the interior of the mw oven itself.
It's a bit similar to 'the nitrostyrene was reduced with LAH to yield the phenethylamine' vs a worked-out description on how to get the thing.
hest:
Sorry for the shortness guy’s, but im’ in the lab right now.
First, a modificated mw.oven is not so complicated to construct.
You need a 30cm long and 6cm wide metal pipe, a metal plate (I use a round one with a diam. off 10cm) with a 6cm hole, an mw oven and a ‘hole-drill’
First you solder the pipe to the metal plate (so it look’s like a cylinder glass), then you drill a hole in the inner shell of the oven, stick’s the pipe through the hole, and soldering the plate onto the oven. Then you drill a hole in the outer oven (or throw it away) and put the oven together. That’s it. You can now reflux in your mw oven. (look at my nice drawing, any funny comment’s wont bee accepted)
hest:
And by the way. The 10g reaction wasen't so violent. I'm sure I could have run it in a normal mw.oven. Just turn the power off when the mixture begin to boil. (use a bigg glass, you have to bee a bit fast)
kurupira:
500mg indole-3-aldehyde was mixed with 1g nitromethane and 50mg amm.acetate...
...from the cold nitroethanesolution an rextalised from methanol ...
...Doesn't the nitromethane boil off when...
--- End quote ---
it's nitroethane, right? ;)
hest:
Yes it is. Silly mee (lol)
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