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Al/Hg Reductive amination under pressure results

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Organikum:
Al/NaOH is my method of choice too, but not with Al-powder/NaOH premixed but with chunks of scrap-aluminium thrown into concentrated lye and sealing the vessel. Evolution of hydrogen can be controlled by temperature, some caustic fumes coming over dont matter in this reaction as long a slight excess of amalgamated aluminium is used.

But thats still a work in progress.  :)

Organikum:
I think its a good idea to add this link to the thread:
Post 187921 (missing) (xtaldoc: "Re: presurrised reductive amination", Chemistry Discourse)

done.

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