The Vespiary

The Hive => Chemistry Discourse => Topic started by: blaztoff on December 24, 2001, 09:11:00 AM

Title: Reacting unreacted
Post by: blaztoff on December 24, 2001, 09:11:00 AM
Can you animate youre safrole from a previous run that you got back during distillation. I ended up recovering the majority of safrole from a failed 02 wacker run. Fairly Possitive very pure still has all the right taste smell.The )2 wacker basically didnt eat up hardly any 02 and i only got very small ketone. Wondering if you can try to reuse it or does it lose its stuff.
Title: Re: Reacting unreacted
Post by: Chromic on December 24, 2001, 10:04:00 AM
Redistill the forerun from the distillation to make sure it is coming over at the correct temperature, and then go ahead and use it.