Author Topic: Reacting unreacted  (Read 1850 times)

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blaztoff

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Reacting unreacted
« on: December 24, 2001, 09:11:00 AM »
Can you animate youre safrole from a previous run that you got back during distillation. I ended up recovering the majority of safrole from a failed 02 wacker run. Fairly Possitive very pure still has all the right taste smell.The )2 wacker basically didnt eat up hardly any 02 and i only got very small ketone. Wondering if you can try to reuse it or does it lose its stuff.

Chromic

  • Guest
Re: Reacting unreacted
« Reply #1 on: December 24, 2001, 10:04:00 AM »
Redistill the forerun from the distillation to make sure it is coming over at the correct temperature, and then go ahead and use it.