The Hive > Chemistry Discourse

very OTC Amph et MethAmph synths

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acx01b:
after reading:
https://www.thevespiary.org/rhodium/Rhodium/chemistry/benzylchloride.html
https://www.thevespiary.org/rhodium/Rhodium/chemistry/meth.phenylacetaldehyde.html

Toluene is refluxed with dried Ca(ClO)2 to yield BenzylChloride by decantation

Benzylchloride is reacted with Magnesium in very dried diethylether and 2-3mg of iodine to yield BenzylMagnesium Chloride

Acetone is reacted with Ethylamine and microwaved-powdered MgSO4 to yield by phase decantation AcetoneEthylimine

AcetoneEthylimine and BenzylMagnesium Chloride are refluxed to yield after hydrolysis Alpha-Methyl-N-Ethyl-amphetamine (methamphetamine like)

indole_amine:
Chemistry sounds alright, but N-ethyl-amphetamine is only half as potent as regular amphetamine...


indole_amine

moo:
The product wouldn't be N-ethylamphetamine but N-ethylphentermine.

indole_amine:
I guess for n-ethyl-amphetamine one would have to use rather acetaldehyde instead of acetone. Correct?


indole_amine

acx01b:
it is quite cross-posting but if acetaldehyde is available, this way is cool too:
Ph-CH2-MgCl + CH3CHO --> Ph-CH2-COH-CH3
Ph-CH2-COH-CH3 + H2SO4(90%)/NaCl --> Ph-CH2-CCl-CH3
Ph-CH2-CCl-CH3 can be extracted very easily (phase separation, toluene should work)
then it is reacted with hexamine (pharmacy store)

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