The Vespiary

The Hive => Methods Discourse => Topic started by: pablos on June 30, 2004, 04:38:00 AM

Title: DMSO autoxidation
Post by: pablos on June 30, 2004, 04:38:00 AM

Have anyone already tried the autoxidation of anethole with dmso?
The procedure papers give exellent yeld (77%) of ketone in only 8
hours at 120 grad.
I have 25 grams pure anethole at home and 100 ml dmso but I can´t find  the ratio in this papers  and I speak not japans.Any good idea?

Title: We are not mind-readers.
Post by: Rhodium on June 30, 2004, 05:04:00 AM

We are not mind-readers. Use the post linking feature.

Title: sorry
Post by: pablos on June 30, 2004, 10:21:00 AM

Sorry I tought it was a well known document.

https://www.thevespiary.org/rhodium/Rhodium/pdf/isosafrole.dmso.oxidation.pdf (https://www.thevespiary.org/rhodium/Rhodium/pdf/isosafrole.dmso.oxidation.pdf)

this is the paper in japan