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but how can i seperate both of the tryptamines ?
is there a known solvent in which one of them will desolve and the other won't ?do i have to do a fractinal crystalisation ?
thank so much
Waldo
probably the same answer....
-------------------the good reverend drone
Ipsa scientia potestas est
Strong basic conditions will convert hydroxy-tryptamines into the respective phenolates (indolates!?). But these are highly unstable in the presence of oxygen and immediately form dark polymeric degradation products (blueing reaction of psilocin!).
Acidic column chromatography would be a solution (e.g. silica gel 0.05 - 0.2 mm (coarse graduation!!!) solvent isopropanol:acetic acid:H2O 20:6:3 as a starting point for further optimization)