Could Sodiumdichromate replaced with potassiumdichromate
without any consequences in that Codeine to
14-Hydroxycodeinone synth?
https://www.thevespiary.org/rhodium/Rhodium/chemistry/oxycodone2.html (https://www.thevespiary.org/rhodium/Rhodium/chemistry/oxycodone2.html)
Then swim would like to know if Dibrommethan could make
the same job instead of methansulfonic acid (Tribrommethan)in the further Oxymorphone synth?
Swim was very happy if some bee out there could answer
this question.
Maybe dope_amine hisself made experience in that case,
but any other suggestion will be welcome of course. :)
There isn`t much info out here in the Hive about
this unpopular synth.
It seems that we are the only two at this time.....
There is also a thread in the Methods Dicourse,
which of course uses other synth routes and chemicals. Maybe you take a look at it.
However by searching the Hive I found Bulldog44`s 2 years old posts.
Post 256825 (https://www.thevespiary.org/talk/index.php?topic=9854.msg25682500#msg25682500)
(Bulldog44: "Need help.", Methods Discourse)
Post 267113 (https://www.thevespiary.org/talk/index.php?topic=9551.msg26711300#msg26711300)
(Bulldog44: "Re: So what the hell is it ??", Methods Discourse)
He did a nano with about 0.5 g starting codi.
Two month later he said he didn´t have lot success.
Post 300426 (https://www.thevespiary.org/talk/index.php?topic=9664.msg30042600#msg30042600)
(Bulldog44: "update", Methods Discourse)
I will give it a try with about 3g.
You said the solubility is pretty important.
What do you think how much water is necassary
for 2g K2Cr2O7?
Since the Potdichrom. has a very less solubility
than NAdichrom. About 5g/100ml H2O.
I would try it with 2g and 50ml water.
Or what do you think? Would the increasing of water amount
harm the synth in any way