The ISO won't dissolve whole pills like that,
This is a joke right? The pills act almost identically in dry iso, 99% iso, and 97%iso. they bubble, shells split there is some swelling. They fall apart much like a cookie in milk, leaving the shells in un-dissolved flakes. When any lower percentage is used one will note the pills sticking to each other. In addition, more swelling per water in the mix. I will not entertain this any further.....
Also what can happen is that unbasified pfed can exist in the non polar used to extract.
unbasified pfed?exist in nonpolar?
Ok I am sure you are posting this to be helpful, so I will change my tone here. I will not ask for proof but I invite you to check this part.
As for the swelling a all, HELLO and thank you for joining us, please refrain from commenting unless you are sure what page we are on! Oh and see Geez for "Posts, Grammar and comprehension 101", I did!
hot dry n fast gives that stuborn ass oil reaction that has to be heated to mars (mark here) or mixed with another .75 rp added by a little DH20 then coax it into a boil followed by a bit more I2 and more water, top with restrickted access condencer and crank it up to a hard boil very wet at this point. After about 30-45 min clears up a bit and I2 releases into condencer.
Come on man, either do the push/pull right, or opt for the LWR. A condenser is not needed in a proper push/pull setup, however it is the heart of a reflux. If you want to master the push/pull read up on posts by Jacked and Worlock.
Of course you could just skip all the b.s. and reflux that stuff for 24hrs for the same product every time. What is the big rush. Hell, you could adjust water ratios and shoot for a 12 hr. reflux, if time is the problem.
With as much time as swiw has put into his/her pill extraction techniques, a better reaction method (i.e. LWR), would certainly up your yeild and purity of product.