Author Topic: New use for the leftovers from sas distilling. - gyrogearloose  (Read 1407 times)

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          [Image][Image]  New use for the leftovers from sas distilling.

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   Author        Topic:   New use for the leftovers from sas distilling.

   gyrogearloose [Image] posted 01-09-99 04:27 AM
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                 --------------------------------------------------------
                 Last post here for me.
                 I know someone will spit on this but here goes anyway.
                 In the recent past I discovered that if you saver the
                 leftovers from distillation of sassafras you can use it
                 to distill the ketone without burnt stuff leftover, it
                 works better than cooking oil or peanut oil(tried both)
                 you can use it over and over and over.
                 Well now shit on it as fast as you can.
                 Bye.

   ChemHack      [Image] posted 01-09-99 09:26 PM
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                 When distilling safrole I am often left with a thick
                 darkBrownBlackish gunk. Is this the stuff you are
                 talking about?

                 Sometimes during safrole distillation some of it gets
                 charred onto the boiling flask. If you re-use the
                 leftovers in this way will the charring also happen or
                 does it only happen the first time when doing the
                 safrole? (ie all that can char does char)

                 I take it that it has a bp that is higher than the
                 ketone as well....

                 I suppose you could also use it if you were gonna
                 distill the freebase amine at the end...

                 Whadda ya think?

   ChemHack      [Image] posted 01-09-99 09:28 PM
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                 PS: I hope you don't think that I am shitting on your
                 idea. I like it.

   gyrogearloose [Image] posted 01-11-99 04:35 AM
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                 Nah, I don't think you are shitting on it, as for me
                 When I distill it I don't go quite that far to end up
                 with dark brown stuff I stop as soon as the temp in the
                 top of vageraux colmn gets higher than safrole temp,
                 thus I am left with a little darl yellow stuff each
                 time and I add it to a supply of it and then use it to
                 distill ketone over without charring. It does boil
                 higher, all those things that don't come over fast.
                 beats cooking oil or cottenseed oil for me anyway. I
                 even use it to distill over iso sometimes same
                 results......
                 Standard disclaimer here#####
                 you know don't try this at home, it may be against the
                 Law, you could get hurt, you don't have a note from
                 your Mom, only ment to entertain. or amuse.

   ChemHack      [Image] posted 01-11-99 01:42 PM
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                 I doubt that this would work very well for the oil that
                 I currently use. The reason is that there does not seem
                 to be a clear "break" in the boiling point.

                 For example: At atmospheric pressure it begins to boil
                 about 232C but the temp continues to rise as clear
                 safrole comes over. The contents of the distilling
                 flask get darker and darker and by the time it hits
                 245C only a black oil remains. I imagine that if
                 heating was continued that the temp would continue to
                 slowly rise as the shit got thicker and thicker and
                 finally charred.

                 So, even if I leave that "other" stuff behind when
                 distilling safrole, it will likely come over anyway
                 when distilling higher boiling oils like iso-saf or
                 ketone.

                 I really like your idea, I just don't think it would
                 work very well for me any my particular oil....

   gyrogearloose [Image] posted 01-15-99 02:57 AM
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                 See me for good oil......

   Stonium       [Image] posted 01-15-99 07:20 AM
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                 gyrogearloose: You said: "See me for good oil."

                 OK, how do I that? email: stonium@hotmail.com

                 Muchas Gracias,
                 Stonium

   Methyl Man    [Image] posted 01-15-99 05:38 PM
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                 Mr. Gyrogearloose: would you mind imparting that info
                 to me as well?
                 b_marapuna@hotmail.com (no, it's not my real name!)

                 thanx
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