Author Topic: TS@ #2 rxn reduction time.  (Read 1411 times)

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dormouse

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TS@ #2 rxn reduction time.
« on: April 19, 2000, 05:00:00 AM »
Author  Topic:   TS@ #2 rxn reduction time. 
Arthur Bach
Member   posted 10-23-98 02:51 AM          
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I don't think I really belong in this forum yet, but the other Bees refered me here for a posibble answer to this question.
If someone was to follow TS2 and scale up #2 5x, can the rxn be performed at 60-70c with a 6 liter three necked flask, reflux condenser and thermometer to reduce the rxn time ? Is there another way to reduce the stirring sime ?


Arthur Bach
Member   posted 10-25-98 06:58 PM          
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Aparrently no one knows. Does anyone have a ideas to reduce the rxn time from 72 hours ?