Swim's previous attempt with this method worked however the vigorous reaction that was supposed to occur didn't. 2000ml of distilled safrole was placed in a 5L flask equipped with a thermometer and condenser. 10g Fe(CO)5 and 6.5g NaOH both ACS grade were then added. Solution immediatley took on a grennish/yellow color that turned a dark grennish/black color with heating. Solution was heated to 110 (no vigorous reaction) heating was continued up to 160 degrees. Resulting organic mixtures was distilled at 135-137 degress leaving a very slightly clear yellow oil. This was the only fraction to come over. When used in the performic it without a doubt produced MDP2P. Does anybody have any experience with this method? I know raflike did however it seems he is no longer part of the board. Swim is weary of using 15L safrole with this method, however, just KOH will take forever.