The Vespiary

The Hive => Methods Discourse => Topic started by: RollWitMe on March 31, 2001, 09:29:00 AM

Title: MDE via Al/Hg Nitro
Post by: RollWitMe on March 31, 2001, 09:29:00 AM
SWIM followed MM writeup and threw in some nitroethane instead of nitromethane, 25ml's instead of 20. The reaction went really smooth didnt choke the condensor at an addition rate of 3-4 drops per second. 25g of ketone was used, 30g Al, allowed to spin for 2h after addition was finished. basified, extracted, washed, dried and gassed to get a little over 20g of the hydrochloride. SWIM isĀ  sure you all already knew this but what the heck, boredom struck and SWIM felt like typing it out anyways :(


I like to cook!
Title: Re: MDE via Al/Hg Nitro
Post by: Dr_Sister on April 02, 2001, 08:15:00 AM
8)  did you make or buy the nitroethane?
Title: Re: MDE via Al/Hg Nitro
Post by: RollWitMe on April 02, 2001, 10:41:00 AM
the neighbors cat sorta bought it for company reasons, in excess, NitroE was tested and Xtra basically given to the cat. cats are evil i tell you! evil!


I like to cook!