Successful Long Wet Reflux
E=11.5gms
MBRP=8.625gms
I2=13.8gms
DH20=11.5ml
SWIGS added the DH20 then the MBRP then the I2 then finally the E. In a later message from an elderbee he was instructed to mix the water, e, and red then add the I2. The flask would then heat a little at most. But SWIGS did something different, which may contribute to by products being formed. Not only did he add the reactants in the wrong order but he added them to an already warm flask. The inner
Gflask temp was 75°C-80°C.
The reactants were added to the 237ml
Gflask in the
Goil bath in this order: DH20 MBRP I2 the sound of very small sizzling steaks and some wafts of white smoke were observed. The E was added…still more smoke, not an overwhelming amount of smoke but definitely enough to notice. I am not sure if it mattered but the temp in SWIGS’s
Glab was around 45°F The
Gcondenser was fit with teflon tape on the end in the
Gflask and the other end fit with a punchball balloon prior to weighing the reactants. The condenser was placed into the end of the flask and taped with electrical tape. The condenser was suspended from the ceiling with a coat hanger at just the right height.
At hour 14 the heat was turned up to 105°C
I DON’T KNOW WHY At hour 16 the reaction fluid was observed as having two layers the top being as red as blood the bottom being orangish looking and murky but more translucent than the top. Upon further investigation and better lighting it was found that the bottom layer was comprised mostly of MBRP and a clearish fluid and the top layer was blood red.
At hour 36 After consulting with an elder bee it was determined that the inner
Gflask temperature was too low (as it was being measured from OUTSIDE the Gflask) and it was CRANKED UP from the suggested 95°C – 97°C mark to 120°C in order to get that inner
Gflask temp up to the desired temp….and at hour twenty-four up to 140°C so that the inner
Gflask temp was closer to 120°C. Bubbling noises were heard at the end of the
Gcondenser, and HI was detected by the nasal apparatus.
At exactly hour 48 the heat was cut off and approximately 12ml of dh20 was heated to boiling and added to the solution. The solution was then swirrrrllllled and observed. MBRP fell like bricks to the bottom of the solution. SWIGS was nervous. He was remembering his last post reaction and how most went onto the floor and he was thinking VERY clearly. (no Icehouse, NO GANJA) He turned the heat back on a bit and let the fluid boil for about ten minutes to clear the excess Iodine then CAREFULLY swirrlllled then poured his precious reaction fluid into his charmin plugged funnel.
When all the reaction fluid had filtered he pulled the plug and squeezed the extra juice out into the collection vessel. SWIGS then filtered again through a new charmin plugged funnel when all was filtered he poured the fluid CAREFULLY into a bottled water bottle with a pop top lid on it and commenced washing his reaction fluid with an equal amount of xylene…and again….and again.
SWIGS then added clean xylene to his reaction fluid…about the same volume as the fluid then started basing with 20-30% lye solution very carefully…a few drops at a time swirl drop swirl and on and on till wham! Milky white to stay…..SWIGS gave it about 10 minutes and sepped the based fluid and xylene keeping the xylene in another bottled water bottle. SWIGS added xylene twice more and and on the last time sat down to have a smoke. (In another room). SWIGS was feeling great at this point and decided it was time to wash his np.
First he warmed some DH20. then he poured that into his np/meth and shook tha fuck outta it. SWIGS walked away and had a smoke and half a beer. Came back sepped off the water into a clean water bottle and added more DH20 to the np/meth….and then again….The water SWIGS sepped off the last time didn’t feel slick or anything so he opted to proceed to the final step before evapping.
So he added half the volume of water as np/meth then added 5 to 7 drops of 31% muriatic acid and shook da fuck outta it. Gave it 10 minutes and another half a beer, sepped the water off into the evap dish and did it again adding 4 drops of muriatic, then a third time with no more acid.
Finally the hotplate was turned on to medium heat and the water/meth was evapped down to an almost solid and just before the last of the water evapped it was flooded with cold dry acetone….bubble bubble toil and trouble….all the acetone evapped off nearly immediately and what was left was about 7gms of yellowish sparkly powder. Smoked nice….When dissolved in water and consumed the effect was ALOT MORE PROFOUND AND I DO MEAN ALOT.
Warning This shit is fucking potent. Maybe 10 times what SWIGS is used to so don’t bee a dumbass like SWIGS and eat a whole gm and a half at once or you might end up cooking on a much higher plane. Like yer next life.Once again…Thanks geez, ici, mr_p, ware, SHORTY, RHODIUM
The disclaimer. Nothing typed in this document is true except what I say is true and I say none of it is true. It's all something I made up to get attention from my peers. I don't know any of the users in this forum so nobody mentioned here did shit to help me do nothing I didn't do....So If you are L.E. GOINFUCKINYERSELFINDABATHROOMWITYERMUDDERSDILDO,MMMMMMK?. And DAMMIT! I'm sorry I beat the fuck outta you in high school...Well not really it was kinda fun. Oh and I'm sorry I fucked your sister too. No. I really am sorry for that, she gave me the clap. Sheethead!