Hmm, ok, SWIM finally got off his ass and decided to distill the mixture. It hasn't even really been in any sunlight for the past day or two, and SWIMS pretty sure all the acetone added evaporated.
SWIM setup for distillation, using his vigeruax (sp?) column thingy, and graham condensor. Upon distillation, my suspitions about the acetone evaping all off were proved to be true. The temp proceeded straight to ~64 or so, and stayed their quite a while. About 64-68 the first main fraction was collected (although their really wasn't any definite separation between fractions, it just slowed a bit and temp rose, until next), which was considered to be methanol and toluene/methanol azeotropes. This smells like a hellacious methanol/toluene mix. The next was like 70-74 or so (this was definitely ethanol/toluene mix, which also lasted a while), and after that somewhere around 80. The temp never rose above 80.
The last fraction was the only one SWIM might be iffy about it containing any suspected P2Pol. SWIM stopped distilling by this time, as there was only a sliver left in the still flask. SWIM figured everything else should have distilled over by now, so whatever sliver was left had to be SOMETHING.
WELL the good news is, it is SOMETHING, but SWIM doesn't know what just yet (some tests are in order). SWIM collected about 10mL of a substance that still has a slight alcohol smell, but no smell like toluene at all.
The liquid has a very very VERY slight tinge of what SWIM thinks is sea green? Maybe a small hint of amberness, but oh so faint. The smell is like burning fucking rubber, mixed with that strange electronics smell, and the bite of alcohol.
SWIM is going to do some tests, and post what comes about.
By the way:
DOes P2Pol form an azeotrope with methanol, ethanol, acetone or toluene?
Also, if this did work, 10mL of the alcohol starting from like almost 400mL worth of shit is sorry as hell. But SWIM would have done bettet with better light, as well as having it long enough to react well. Not cloudy or indirect sunlight for few hours each day. Also if care was taken to seal the flask better, SWIM noticed by the end pretty much all acetone was gone, and that is detrimental to the reaction (yes SWIM read through the patent), so that was probably a killer too.