OK, so swim did a reductive amination with 50 g ketone, 50mL 40% aq. methylamine, 25 g foil, etc. He did it as per Osmium/Brightstar's writeup. However, when the rxn finished and he basified, he was left with a grey solution. Great. Sounds about right. He added 400 mL clear toluene to the solution and left it stirring for 4 hours (he had to go do something important). When he came back he had a orangish solution! No layers! So he added some salt and shook in a sep funnel. Now he got a light orange toluene layer, huge oil droplets (emulsion?) in the interface, and a darker orange water layer. What should he do next? He is especially confused as to the very noticeable color change.