The Hive > Tryptamine Chemistry
Optimum drying temperature for LSA?
luminescent:
Can anyone here give any specifics on the optimum drying temperature for LSA under 30'hg reduced atmos?
Lilienthal:
RT
armageddon:
As low as possible (depends on how much time you can spare for the drying step; lower temp. = more time = more gentle drying).
Greetz, A
luminescent:
Vacuum was first turned on to 30"hg then vacuum oven was turned on and heated up to 90C over a 5 hour period then turned off.Waiting till oven temp cools to 25-30C then slowly equalizing threw bleed valve.Then weighed.
armageddon:
Too much heat. Try 30-40°C next time to avoid partial decomposition. The "heat" function is mainly for hard-to-dry compounds, not sensitive ones!
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