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sudo sulfate containing paracetamol

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jemma_jamerson:
swim has a funny back yard 'cook' story, but this may not bee as simple to resolve as it proberly can beee by the info swim has to tell.. here goes

swim was given a rather large bag of what he was told was sudo sulfate that may have paracetamol in them

UTFSE ofcause would yeild the fact of

1)Lots of hot, dry acetone, and I suggest an a/b extraction method.

or thanks to placebo the immortal

2)Just do a couple of solvent washes, (turps/toluene) to remove povidone and other adulterants that prevent an A/B. Then A/B to leave the paracetamol behind. Finally an acetone wash, or acetone at the start after turps and tol.

3) or basically a dry acetone boil will get rid of most of the paracetamol, just as it does with antihistamines. Maybe just a bigger volume than a boil to remove antishitamines. Making the acetone nice and hot should ensure all of it comes across and gets outta your face.

swim wonders since the back yard boys dont even know for sure what is in them what would be the best advice for this.

swim has a white pill mass with out swims finger prints on the  ;)

wareami:
Howdy Mate!
Ibee thinks Stoni posted the merck info for this a while back which helped superassman come to the conclusion that acetaminophen is soluable in acetone. All bees know that pfed and meth are not.
Check out some of the other solubility characteristics.
Why not start with removing all traces of the pain reliever and then you'll bee left with a pill mass to apply VideoEditors S2E method.
Just a suggestion that makes sense-a-million to The Kidz!

Monograph Number:  48
Title:  Acetaminophen
CAS Registry Number:  103-90-2
CAS Name:  N-(4-Hydroxyphenyl)acetamide
Additional Names:  4¢-hydroxyacetanilide;  p-hydroxyacetanilide;  p-acetamidophenol;  p-acetaminophenol;  p-acetylaminophenol;  N-acetyl-p-aminophenol;  paracetamol
Trademarks:  Acamol (Teva);  Acetalgine (Streuli);  Alpiny (SS Pharm.);  Anaflon (SKB);  Anhiba (Hokuriku);  Apamide (Bayer);  Ben-u-ron (Bene-Arzneimittel);  Calpol (Warner-Lambert);  Captin (Krewel);  Dafalgan (UPSA);  Datril (Bristol-Myers Squibb);  Dirox (Sanofi Winthrop);  Disprol (Reckitt & Colman);  Doliprane (RPR);  Dolprone (Bottu);  Enelfa (Dolorgiet);  Febrilex (Raven);  Gelocatil (Gelos);  Hedex (SKB);  Momentum (Much);  Ortensan (Cimex);  Pacemol (Gemballa);  Panadol (SKB);  Panaleve (Pinewood);  Panasorb (SKB);  Panodil (SKB);  Paraspen (Fisons);  Pasolind N (Stada);  Salzone (Wallace);  Tabalgin (Berk);  Tapar (Parke-Davis);  Tempra (Mead Johnson);  Tylenol (McNeil);  Valadol (Bristol-Myers Squibb)
Molecular Formula:  C8H9NO2
Molecular Weight:  151.16. 
Percent Composition:  C 63.57%, H 6.00%, N 9.27%, O 21.17%
Literature References:  Prepn from p-nitrophenol:  Morse, Ber. 11, 232 (1878); Tingle, Williams, Am. Chem. J. 37, 63 (1907); from p-aminophenol:  Lumière et al., Bull. Soc. Chim. France [3] 33, 785 (1905); Fierz-David, Kuster, Helv. Chim. Acta 22, 94 (1939); Wilbert, De Angelis, US 2998450 (1961 to Warner-Lambert); Bergmann, DE 453577; Chem. Zentr. 1928, I, 2663; Frdl. 16, 238; from p-hydroxyacetophenone hydrazone:  Pearson et al., J. Am. Chem. Soc. 75, 5907 (1953).  Toxicity data:  G. A. Starmer et al., Toxicol. Appl. Pharmacol. 19, 20 (1971); D. C. Dahlin, S. D. Nelson, J. Med. Chem. 25, 885 (1982).  Evaluation of renal effects:  D. P. Sandler et al., N. Engl. J. Med. 320, 1238 (1989).  Comprehensive description:  J. E. Fairbrother, Anal. Profiles Drug Subs. 3, 1-109 (1974).  Review of pharmacology:  B. Ameer, D. J. Greenblatt, Ann. Int. Med. 87, 202-209 (1977).  Review of acetaminophen-induced hepatotoxicity:  J. A. Hinson, Rev. Biochem. Toxicol. 2, 103-129 (1980); idem, Life Sci. 29, 107-116 (1981); and proposed protective agents:  M. Davis, Sem. Liver Dis. 6, 138-147 (1986).  For proposed toxic metabolite see Acetimidoquinone.
Properties:  Large monoclinic prisms from water, mp 169-170.5°.  d421 1.293.  uv max (ethanol):  250 nm (e 13800).  Very slightly sol in cold water, considerably more sol in hot water.  Sol in methanol, ethanol, dimethylformamide, ethylene dichloride, acetone, ethyl acetate.  Slightly sol in ether.  Practically insol in petr ether, pentane, benzene.  LD50 in mice (mg/kg):  338 orally (Starmer), 500 i.p. (Dahlin, Nelson).
Melting point:  mp 169-170.5°
Absorption maximum:  uv max (ethanol):  250 nm (e 13800)
Density:  d421 1.293
Toxicity data:  LD50 in mice (mg/kg):  338 orally (Starmer), 500 i.p. (Dahlin, Nelson)
Use:  Manuf azo dyes, photographic chemicals.
Therap-Cat:  Analgesic; antipyretic.

Peace of the reaction

Have FUN-Bee SAFE

beez_neez:
paracetamol is soluble acetone; 1part paracetamol to 13 parts acetone.
Stick to this ratio and using HOT tone, should see you right.
Assuming that you are an ozbee, Swibn has yet to come accross pills here that have pseudo sulfate and paracetamol.
The only paracetamol pills he has seen are the hcl type.
The sulfate pills that are easy to come by here have the maleate anti-histamine but as we know, this pesky monster is easily overcome.
lots of orange gakk though.

jemma_jamerson:
hailz mate, got an idea that thats all they have in them, surpose i should start with normal acid base , then doil the acetone wash/boil then,

see if they come through the rxn okay.

its a fucking mystry what else could bee in them but swim thinks that thats the only things

beez_kneeez, swim is an ozy bee, im told these are heron brand , and came through blue in the rxn and are a sulfate

blue gakk could freakin mean any thing :P

beez_neez:
If the pills are/were blue, then chances are that they are the d*****n type with the anti-histamine.
let me know how you go with your a/b, as swibn has had poor yields with his method of extracting with these sulfate pills.

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